A practical total synthesis of (+/-)-cermizine D and a formal synthesis of (+/-)-cermizine C
Shi, Xin1,2,3; Bao, Ying1,2,3; Deng, Zhen-Tao1,2,3; Zhu, Yu2,3; Shao, Li-Dong2; Zhang, Hong-Bin1; Zhao, Qin-Shi2
2018-06-01
发表期刊JOURNAL OF CHEMICAL RESEARCH
ISSN1747-5198
期号5页码:274-279
摘要A practical total synthesis of (+/-)-cermizine D and a formal synthesis of (+/-)-cermizine C were achieved. The four-step total synthesis comprised mainly a Michael addition, a Weinreb amide-activated substitution and a sequence of ketalation/PtO2-catalysed dearomatisation/reductive amination reactions that resulted in ring closure in 13.7% overall yield. The formal synthesis was accomplished in 29.7% overall yield.
关键词Cermizine c Cermizine d Total Synthesis Michael Addition Reductive Amination
语种英语
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文献类型期刊论文
条目标识符http://ir.kib.ac.cn/handle/151853/61421
专题植物化学与西部植物资源持续利用国家重点实验室
作者单位1.Yunnan Univ, Sch Chem Sci & Technol, Minist Educ, Key Lab Med Chem Nat Resources, Kunming 650091, Yunnan, Peoples R China
2.Chinese Acad Sci, Kunming Inst Bot, State Key Lab Phytochem & Plant Resources West Ch, Kunming 650201, Yunnan, Peoples R China
3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
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Shi, Xin,Bao, Ying,Deng, Zhen-Tao,et al. A practical total synthesis of (+/-)-cermizine D and a formal synthesis of (+/-)-cermizine C[J]. JOURNAL OF CHEMICAL RESEARCH,2018(5):274-279.
APA Shi, Xin.,Bao, Ying.,Deng, Zhen-Tao.,Zhu, Yu.,Shao, Li-Dong.,...&Zhao, Qin-Shi.(2018).A practical total synthesis of (+/-)-cermizine D and a formal synthesis of (+/-)-cermizine C.JOURNAL OF CHEMICAL RESEARCH(5),274-279.
MLA Shi, Xin,et al."A practical total synthesis of (+/-)-cermizine D and a formal synthesis of (+/-)-cermizine C".JOURNAL OF CHEMICAL RESEARCH .5(2018):274-279.
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