Rapid synthesis of ismine, a bioactive amaryllidaceae alkaloid
Guo, Jing-jing1,2; Yang, Bi-juan2,3; Jing, Chen-xu2; Chen, Duo-zhi2; Hao, Xiao-jiang2
2017-04-01
发表期刊JOURNAL OF CHEMICAL RESEARCH
ISSN1747-5198
期号4页码:202-204
摘要Ismine (6-[2-( methylamino) phenyl]-1,3-benzodioxole-5-methanol, 1), a biologically active alkaloid, has been synthesised by a rapid and simple four-step sequence. This synthesis involved a consecutive aryl-aryl and N-aryl coupling, leading to a phenanthridine derivative in a one-pot sequence, which employed a palladium catalyst and trifurylphosphine as the ligand. This synthesis gave an overall yield of 23%.
关键词Amaryllidaceae Alkaloid Palladium Catalyst Aryl-aryl Coupling N-aryl Coupling
语种英语
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文献类型期刊论文
条目标识符http://ir.kib.ac.cn/handle/151853/60632
专题植物化学与西部植物资源持续利用国家重点实验室
作者单位1.Yunnan Univ Tradit Chinese Med, Coll Tradit Chinese Med, Kunming 650500, Yunnan, Peoples R China
2.Chinese Acad Sci, State Key Lab Phytochem & Plant Resources West Ch, Kunming Inst Bot, Kunming 650201, Yunnan, Peoples R China
3.Yunnan Univ, Sch Chem Sci & Technol, Kunming 650000, Yunnan, Peoples R China
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Guo, Jing-jing,Yang, Bi-juan,Jing, Chen-xu,et al. Rapid synthesis of ismine, a bioactive amaryllidaceae alkaloid[J]. JOURNAL OF CHEMICAL RESEARCH,2017(4):202-204.
APA Guo, Jing-jing,Yang, Bi-juan,Jing, Chen-xu,Chen, Duo-zhi,&Hao, Xiao-jiang.(2017).Rapid synthesis of ismine, a bioactive amaryllidaceae alkaloid.JOURNAL OF CHEMICAL RESEARCH(4),202-204.
MLA Guo, Jing-jing,et al."Rapid synthesis of ismine, a bioactive amaryllidaceae alkaloid".JOURNAL OF CHEMICAL RESEARCH .4(2017):202-204.
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