Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide
Chen, Gang1; Tang, Ying1; Zhang, Qun-Zheng1; Meng, Mei1; Hao, Xiao-Jiang2
2011-02-01
发表期刊JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN1074-1542
卷号41期号:2页码:251-254
摘要(S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide was synthesized from Cbz-l-proline through two steps and characterized by NMR and MS. The crystal structure was determined from single-crystal X-ray diffraction data. It crystallizes in the monoclinic space group, P2(1), with unit cell dimensions a = 7.284(6) angstrom, b = 10.262(9) angstrom, and c = 7.975(7) angstrom, alpha = 90.00 degrees, beta = 114.451(14)degrees, gamma = 90.00 degrees and Z = 2. The absolute configuration of the chiral center is determined as S. In the crystal structure, intermolecular and intramolecular hydrogen bonds are responsible for the formation of a 1-dimensional network.
关键词L-proline (s)-n-(2-hydroxyphenyl) Pyrrolidine-2-carboxamide X-ray Structure
资助信息Shaanxi Science and Technology Department[SJ08B20]; Shaanxi Education Department[09JK702]
学科领域Crystallography ; Spectroscopy
DOI10.1007/s10870-010-9935-z
收录类别SCI
语种英语
WOS研究方向Crystallography ; Spectroscopy
WOS类目Crystallography ; Spectroscopy
WOS记录号WOS:000286469800030
引用统计
文献类型期刊论文
条目标识符http://ir.kib.ac.cn/handle/151853/5355
专题植物化学与西部植物资源持续利用国家重点实验室
作者单位1.Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Shaanxi, Peoples R China
2.Chinese Acad Sci, State Key Lab Phytochem & Plant Resources W China, Kunming Inst Bot, Kunming 650204, Yunnan, Peoples R China
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GB/T 7714
Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,et al. Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide[J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,2011,41(2):251-254.
APA Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,Meng, Mei,&Hao, Xiao-Jiang.(2011).Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide.JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,41(2),251-254.
MLA Chen, Gang,et al."Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide".JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 41.2(2011):251-254.
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