| Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry | |
| Yan, Zhou1,2; Xia, Bing2; Qiu, Ming Hua3; Sheng, Ding Li2; Xu, Hong Xi1 | |
| 2013-11-01 | |
| 发表期刊 | BIOMEDICAL CHROMATOGRAPHY
 |
| 卷号 | 27期号:11页码:1560-1567 |
| 摘要 | A rapid and reliable method was established for simultaneous determination of main triterpenoids in Ganoderma lucidum spores using ultra-high-performance liquid chromatography coupled with triple quadrupole mass spectrometry (UPLC-TQ-MS). The established method was validated in terms of linearity, sensitivity, precision, accuracy and stability, and was successfully applied to determine the contents of 10 main triterpenoids in different batches of G. lucidum spores. The analysis results showed that moderate levels of triterpenoids were found in G. lucidum spores. In addition, a MS full scan with a daughter ion scan experiment was performed to identify the potential derivatives of triterpenoids present in G. lucidum spores. As a result, a total of 22 triterpenoids from different G. lucidum spores were unequivocally or tentatively identified via comparisons with authentic standards and literatures. This method provides both qualitative and quantitative results without the need for repetitive UPLC-MS analyses, thereby increasing efficiency and productivity, making it suitable for high-throughput applications. Copyright (c) 2013 John Wiley & Sons, Ltd. |
| 关键词 | Ganoderma Lucidum Spores Triterpenoid Multiple Reaction Monitoring Daughter Ion Scan Experiment |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000328324100026 |
| 引用统计 | |
| 文献类型 | 期刊论文 |
| 条目标识符 | http://ir.kib.ac.cn/handle/151853/19239 |
| 专题 | 植物化学与西部植物资源持续利用国家重点实验室 |
| 作者单位 | 1.Shanghai Univ Tradit Chinese Med, Shanghai 201203, Peoples R China 2.Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Peoples R China 3.Chinese Acad Sci, Kunming Inst Bot, Kunming 650201, Peoples R China |
| 推荐引用方式 GB/T 7714 | Yan, Zhou,Xia, Bing,Qiu, Ming Hua,et al. Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry[J]. BIOMEDICAL CHROMATOGRAPHY,2013,27(11):1560-1567. |
| APA | Yan, Zhou,Xia, Bing,Qiu, Ming Hua,Sheng, Ding Li,&Xu, Hong Xi.(2013).Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry.BIOMEDICAL CHROMATOGRAPHY,27(11),1560-1567. |
| MLA | Yan, Zhou,et al."Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry".BIOMEDICAL CHROMATOGRAPHY 27.11(2013):1560-1567. |
| 条目包含的文件 | ||||||
| 文件名称/大小 | 文献类型 | 版本类型 | 开放类型 | 使用许可 | ||
| 2013e0023h.pdf（507KB） | 开放获取 | CC BY-NC-ND | 浏览 下载 | |||
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