Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry
Yan, Zhou1,2; Xia, Bing2; Qiu, Ming Hua3; Sheng, Ding Li2; Xu, Hong Xi1
2013-11-01
发表期刊BIOMEDICAL CHROMATOGRAPHY
卷号27期号:11页码:1560-1567
摘要A rapid and reliable method was established for simultaneous determination of main triterpenoids in Ganoderma lucidum spores using ultra-high-performance liquid chromatography coupled with triple quadrupole mass spectrometry (UPLC-TQ-MS). The established method was validated in terms of linearity, sensitivity, precision, accuracy and stability, and was successfully applied to determine the contents of 10 main triterpenoids in different batches of G. lucidum spores. The analysis results showed that moderate levels of triterpenoids were found in G. lucidum spores. In addition, a MS full scan with a daughter ion scan experiment was performed to identify the potential derivatives of triterpenoids present in G. lucidum spores. As a result, a total of 22 triterpenoids from different G. lucidum spores were unequivocally or tentatively identified via comparisons with authentic standards and literatures. This method provides both qualitative and quantitative results without the need for repetitive UPLC-MS analyses, thereby increasing efficiency and productivity, making it suitable for high-throughput applications. Copyright (c) 2013 John Wiley & Sons, Ltd.
关键词Ganoderma Lucidum Spores Triterpenoid Multiple Reaction Monitoring Daughter Ion Scan Experiment
收录类别SCI
语种英语
WOS研究方向Biochemistry & Molecular Biology ; Chemistry ; Pharmacology & Pharmacy
WOS类目Biochemical Research Methods ; Biochemistry & Molecular Biology ; Chemistry, Analytical ; Pharmacology & Pharmacy
WOS记录号WOS:000328324100026
引用统计
文献类型期刊论文
条目标识符http://ir.kib.ac.cn/handle/151853/19239
专题植物化学与西部植物资源持续利用国家重点实验室
作者单位1.Shanghai Univ Tradit Chinese Med, Shanghai 201203, Peoples R China
2.Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Peoples R China
3.Chinese Acad Sci, Kunming Inst Bot, Kunming 650201, Peoples R China
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GB/T 7714
Yan, Zhou,Xia, Bing,Qiu, Ming Hua,et al. Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry[J]. BIOMEDICAL CHROMATOGRAPHY,2013,27(11):1560-1567.
APA Yan, Zhou,Xia, Bing,Qiu, Ming Hua,Sheng, Ding Li,&Xu, Hong Xi.(2013).Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry.BIOMEDICAL CHROMATOGRAPHY,27(11),1560-1567.
MLA Yan, Zhou,et al."Fast analysis of triterpenoids in Ganoderma lucidum spores by ultra-performance liquid chromatography coupled with triple quadrupole mass spectrometry".BIOMEDICAL CHROMATOGRAPHY 27.11(2013):1560-1567.
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