Rapid characterization of chemical constituents in Saniculiphyllum guangxiense by ultra fast liquid chromatography with diode array detection and electrospray ionization tandem mass spectrometry
Geng, Chang-An1; Chen, Hao1; Chen, Xing-Long1; Zhang, Xue-Mei1; Lei, Li-Gong2; Chen, Ji-Jun1
Corresponding AuthorChen, JJ (reprint author), Chinese Acad Sci, Kunming Inst Bot, State Key Lab Phytochem & Plant Resources West Ch, 132 Lanhei Rd, Kunming 650201, Peoples R China. ; chenjj@mail.kib.ac.cn
2014-03-15
Source PublicationINTERNATIONAL JOURNAL OF MASS SPECTROMETRY
ISSN1387-3806
Volume361Pages:9-22
AbstractSaniculiphyllum guangxiense as a highly distinctive species within Saxifragaceae is fallen to the critically endangered category, whose chemical and taxonomic information is still little-known. The first time LC-DAD/MSn investigation on S. guangxiense led to the detection and characterization of 50 compounds, involving cyanogenic glycosides, phenolic sulfates, triterpenoids, amino acids, phenyl-propanoids, aromatic derivatives, lignans, flavonoids, nucleosides, fatty acids and carbohydrate, based on their fragmentation characteristics, UV spectra or comparison with the reference compounds. The collision induced dissociation (CID) fragmentation patterns for several types of compounds were also concluded. The main constituents of S. guangxiense were revealed as cyanogenic glycosides, triterpenoids, phenolic sulfates and organic acids, which were very different from other Saxifragaceae plants. This paper will provide valuable information for understanding its chemical profiles and taxonomic position in Saxifragaceae from a chemotaxonomic point of view. (C) 2014 Elsevier B.V. All rights reserved.
KeywordLc-dad/esi-msn Saniculiphyllum Guangxiense Cyanogenic Glycosides Triterpenoids Phenolic Sulfates
Subject AreaPhysics, Atomic, Molecular & Chemical ; Spectroscopy
DOI10.1016/j.ijms.2014.01.021
Indexed BySCI
Language英语
WOS Research AreaPhysics ; Spectroscopy
WOS SubjectPhysics, Atomic, Molecular & Chemical ; Spectroscopy
WOS IDWOS:000334085200002
Citation statistics
Cited Times:11[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.kib.ac.cn/handle/151853/18042
Collection植物化学与西部植物资源持续利用国家重点实验室
Affiliation1.Chinese Acad Sci, Kunming Inst Bot, State Key Lab Phytochem & Plant Resources West Ch, Kunming 650201, Peoples R China
2.Chinese Acad Sci, Kunming Inst Bot, Key Lab Biodivers & Biogeog, Kunming 650201, Peoples R China
Recommended Citation
GB/T 7714
Geng, Chang-An,Chen, Hao,Chen, Xing-Long,et al. Rapid characterization of chemical constituents in Saniculiphyllum guangxiense by ultra fast liquid chromatography with diode array detection and electrospray ionization tandem mass spectrometry[J]. INTERNATIONAL JOURNAL OF MASS SPECTROMETRY,2014,361:9-22.
APA Geng, Chang-An,Chen, Hao,Chen, Xing-Long,Zhang, Xue-Mei,Lei, Li-Gong,&Chen, Ji-Jun.(2014).Rapid characterization of chemical constituents in Saniculiphyllum guangxiense by ultra fast liquid chromatography with diode array detection and electrospray ionization tandem mass spectrometry.INTERNATIONAL JOURNAL OF MASS SPECTROMETRY,361,9-22.
MLA Geng, Chang-An,et al."Rapid characterization of chemical constituents in Saniculiphyllum guangxiense by ultra fast liquid chromatography with diode array detection and electrospray ionization tandem mass spectrometry".INTERNATIONAL JOURNAL OF MASS SPECTROMETRY 361(2014):9-22.
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