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题名: Stereoselective Synthesis of Diazabicyclic beta-Lactams through Intramolecular Amination of Unactivated C(sp(3))-H Bonds of Carboxamides by Palladium Catalysis
作者: Zhang, Shi-Jin1, 2; Sun, Wen-Wu2, 3; Cao, Pei2; Dong, Xiao-Ping1; Liu, Ji-Kai4; Wu, Bin2, 4
刊名: JOURNAL OF ORGANIC CHEMISTRY
英文摘要: An efficient C(sp(3))-H bond activation and intramolecular amination reaction via palladium catalysis at the beta-position of carboxyamides to make beta-lactams was described. The investigation of the substrate scope showed that the current reaction conditions favored activation of the beta-methylene group. Short sequences were developed for preparation of various diazabicyclic beta-lactarn compounds with this method as the key step from chiral proline and piperidine derivatives.
出版日期: 2016-02-05
卷号: 81, 期号:3, 页码:956-968
DOI标识: 10.1021/acs.joc.5b02532
语种: 英语
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内容类型: 期刊论文
URI标识: http://ir.kib.ac.cn/handle/151853/25957
Appears in Collections:植物化学与西部植物资源持续利用国家重点实验室_期刊论文

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作者单位: 1.Chengdu Univ Tradit Chinese Med, Coll Pharm, Chengdu 611137, Peoples R China
2.Chinese Acad Sci, Kunming Inst Bot, State Key Lab Phytochem & Plant Resources West Ch, Kunming 650201, Peoples R China
3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
4.South Cent Univ Nationalities, Sch Pharmaceut Sci, Wuhan 430074, Peoples R China
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