一种漆酚化合物的制备方法
程永现 ; 陈显强 ; 吕青
Application Number201210085216.3
Rights Holder中国科学院昆明植物研究所
Date Available2012-08-08
Abstract公开了生漆中一种漆酚化合物(Z)-3-(pentadec-8-en-1-yl)benzene-1,2-diol的制备方法,包括将来自漆树的生漆用乙酸乙酯溶解后进行硅胶柱层析,石油醚-乙酸乙酯系统洗脱,HPLC检测并收集含有该化合物的流份,合并洗脱液并减压回收溶剂得浓缩后的油状物,进行RP-18反相柱层析,甲醇-水洗脱,收集含有该化合物的流份,浓缩得到的油状物行Sephadex?LH-20柱层析进行脱色,并除去部分杂质。该工艺操作方便,三步柱层析即可从生漆中获得高纯度和高收率的纯品。工艺中使用的反相硅胶和凝胶材料均可反复使用,洗脱溶剂相对廉价,且可循环使用,适合工业化生产。
Document Type专利
Identifierhttp://ir.kib.ac.cn/handle/151853/16292
Collection植物化学与西部植物资源持续利用国家重点实验室
Recommended Citation
GB/T 7714
程永现,陈显强,吕青. 一种漆酚化合物的制备方法. CN201210085216.3.
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